1: sodium hydride / dichloromethane; mineral oil / 15 h / 20 °C / |Inert atmosphere
2: sodium hydroxide; water / tetrahydrofuran / 18 h / 20 °C
View Scheme
参考文献
Fritz, Sven P.; Matlock, Johnathan V.; McGarrigle, Eoghan M.; Aggarwal, Varinder K.
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 10827 - 10831
1: (SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium / dichloromethane / |Inert atmosphere; |Reflux
2: sodium hydride / dichloromethane; mineral oil / 15 h / 20 °C / |Inert atmosphere
3: sodium hydroxide; water / tetrahydrofuran / 18 h / 20 °C
View Scheme
参考文献
Fritz, Sven P.; Matlock, Johnathan V.; McGarrigle, Eoghan M.; Aggarwal, Varinder K.
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 10827 - 10831
