3-氮杂双环[3.1.0]-6-己基氨基甲酸叔丁酯合成路线 （共 12 条）
反应条件
1.1: water; lithium hydroxide hydrate / methanol / 18 h / 20 °C 1.2: 0 °C / pH ~ 3 2.1: triethylamine; diphenyl phosphoryl azide / 22 h / Reflux 3.1: hydrogen / palladium(II) oxide hydrate / methanol / 2.5 h / 775.74 Torr / Inert atmosphere View Scheme
参考文献
WO2012/125662 A1, ;
WO 2012/125662 A1
反应条件
1.1: sodium hydrogencarbonate / 1,4-dioxane; water 2.1: water; lithium hydroxide hydrate / methanol / 18 h / 20 °C 2.2: 0 °C / pH ~ 3 3.1: triethylamine; diphenyl phosphoryl azide / 22 h / Reflux 4.1: hydrogen / palladium(II) oxide hydrate / methanol / 2.5 h / 775.74 Torr / Inert atmosphere View Scheme
参考文献
WO2012/125662 A1, ;
WO 2012/125662 A1
