N,N-二甲基-3-氧代戊酰胺合成路线 (共 4 条)
反应条件
1: diiodomethane With diethylzinc in hexane; dichloromethane
T=0°C; 0.166667 h;
2: acetoacetic acid dimethylamide in hexane; dichloromethane
T=0°C; 0.25 h;
参考文献
Hilgenkamp, Ramona; Zercher, Charles K
Tetrahedron, 2001 , vol. 57, # 42 p. 8793 - 8800
反应条件
1-bromo-1,1-dimethylethane in diethyl ether
1) -78 grad C, 1.5 h, 2) -78 grad C then to room temperature;
参考文献
Pouilhes, Annie; Thomas, Susan E.
Tetrahedron Letters, 1989 , vol. 30, # 17 p. 2285 - 2288
反应条件
in water; toluene
Heating;
参考文献
Hueerlaender, Doris; Froehlich, Roland; Erker, Gerhard
Journal of the Chemical Society. Dalton Transactions, 2002 , # 7 p. 1513 - 1520
参考文献
Lukes,R. et al.
Collection of Czechoslovak Chemical Communications, 1963 , vol. 28, p. 2182 - 2198