1: With hydrogenchloride in dichloromethane; water T=20°C; 1 h; 2: With sodium hydroxide in dichloromethane; water pH=7; cooling with ice; Product distribution / selectivity;
参考文献
INDIANA UNIVERSITY RESEARCH AND TECHNOLOGY CORPORATION; MCCARTHY, James, R.
Patent: WO2011/137222 A1, 2011 ;
Location in patent: Example 25 ;
1.1: hydrogenchloride / dichloromethane; water / 1 h / 20 °C 1.2: pH 7 / cooling with ice 2.1: dichloromethane; water / 1 h / 20 °C 2.2: pH 9 / cooling with ice View Scheme
参考文献
INDIANA UNIVERSITY RESEARCH AND TECHNOLOGY CORPORATION; MCCARTHY, James, R.
Patent: WO2011/137222 A1, 2011 ;
