反应条件
1.1: acetic acid / water / 12 h / 20 °C / Inert atmosphere
2.1: magnesium sulfate / dichloromethane / 0.08 h / Inert atmosphere
2.2: 5 h / 20 °C / Inert atmosphere
3.1: 15-crown-5; sodium hexamethyldisilazane / tetrahydrofuran / -40 °C / Inert atmosphere
4.1: ammonium cerium (IV) nitrate / water; acetonitrile / 16 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Evans, Caroline D.; Mahon, Mary F.; Andrews, Philip C.; Muir, James; Bull, Steven D.
Organic Letters, 2011 , vol. 13, # 23 p. 6276 - 6279