反应条件
(Z)-9-octadecenoic acid in neat (no solvent) thermal decomp. of Fe(CO)5 in the presence of oleic acid and a small amount of trioctylphosphine oxide with the Fe:acid molar ratio fixed at 1:2.5, 180°C, 130°C grouth temp.; crystals were washed with anhydrous methanol; powder X-ray diffraction;
参考文献
Samia, Anna C. S.; Hyzer, Kylee; Schlueter, John A.; Qin, Chang-Jin; Jiang, J. Samuel; Bader, Samuel D.; Lin, Xiao-Min
Journal of the American Chemical Society, 2005 , vol. 127, # 12 p. 4126 - 4127