in N,N-dimethyl-formamide Ar atmosphere, 25°C, ionic strength 1 M (NaClO4); not isolated; potentiometric monitoring (3 mass-percent indium amalgam indicator electrode), estimation of stability const. of InBr3 in DMF;
参考文献
Sov. Prog. Chem. (Engl. Transl.), , vol. 54/4, p. 1 - 4
Ukrainskii Khimicheskii Zhurnal (Russian Edition), , vol. 54, p. 339 - 342
in N,N-dimethyl-formamide Ar atmosphere, 25°C, ionic strength 1 M (NaClO4); not isolated; potentiometric monitoring (3 mass-percent indium amalgam indicator electrode), estimation of stability const. of InBr3 in DMF;
参考文献
Sov. Prog. Chem. (Engl. Transl.), , vol. 54/4, p. 1 - 4
Ukrainskii Khimicheskii Zhurnal (Russian Edition), , vol. 54, p. 339 - 342
Red'kin, A. N.; Smirnov, V. A.; Makovei, Z. I.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1987 , vol. 32, p. 1756 - 1760
Zhurnal Neorganicheskoi Khimii, 1987 , vol. 32, p. 3030 - 3035
→
反应条件
in neat (no solvent) mixt. of the starting materials heated in evacuated sealed quartz tubes to 500-900°C; decompn. of educts ocurrs, InBr3 sublimates off;
参考文献
Range, Klaus-Juergen; Handrick, Karin
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1988 , vol. 43, # 2 p. 153 - 158
in melt prepd. from stoich. amts. of components, mixt. heated in evacuated, fused quartz ampoule at 570 K for 1 d then cooled down to 470 K (1.5 K/h); InBr3 sublimed;
参考文献
Zeitschrift fur Anorganische und Allgemeine Chemie, , vol. 629, # 3 p. 375 - 380
