1: With n-butyllithium; N,N,N',N',tetramethyl-ethylenediamine in tetrahydrofuran; hexane
T=-76 - 20°C; P=760.051 Torr; Inert atmosphere;
2: With boric acid trimethyl ester in tetrahydrofuran; hexane
T=0 - 20°C;
3: With hydrogenchloride; water in tetrahydrofuran; hexane
T=0°C;
参考文献
Chin, Elbert; Li, Jim; Lui, Albert Sui-Ting; Talamas, Francisco Xavier
Patent: US2010/297073 A1, 2010 ;
Location in patent: Page/Page column 18 ;
2 Pd/C; potassium acetate in 1-methyl-pyrrolidin-2-one; water
T=100°C; 0.333333 h; Microwave irradiation;
参考文献
Singh, Brajendra K.; Cavalluzzo, Claudia; De Maeyer, Marc; Debyser, Zeger; Parmar, Virinder S.; Van Der Eycken, Erik
European Journal of Organic Chemistry, 2009 , # 27 p. 4589 - 4592
