三甲基(2,3,4,5-四甲基-2,4-环戊二烯-1-基)硅烷合成路线 （共 4 条）
反应条件
in tetrahydrofuran T=20°C; 1 h;
参考文献
Krut'ko; Borzov; Veksler
Russian Chemical Bulletin, 2004 , vol. 53, # 10 p. 2182 - 2186
反应条件
1: LiAlH4 2: p-TsOH / benzene / Ambient temperature 3: 1) BuLi, tetramethylethylenediamine / 1) hexane, room temp., 15 h; 2) Et2O, reflux, 3 d View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 69, # 4 p. 661 - 672
反应条件
1: p-TsOH / benzene / Ambient temperature 2: 1) BuLi, tetramethylethylenediamine / 1) hexane, room temp., 15 h; 2) Et2O, reflux, 3 d View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 69, # 4 p. 661 - 672
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine 1) hexane, room temp., 15 h; 2) Et2O, reflux, 3 d; Yield given. Multistep reaction;
参考文献
Canadian Journal of Chemistry, , vol. 69, # 4 p. 661 - 672
