反应条件
in neat (no solvent) byproducts: MgCl2; vac. or N2 filled glove box; mixt. grinding, heating in evac. sealed quartz ampoule at 850°C for 10 h, cooling to room temp., grinding; powder trituration with MeOH or H2O;
参考文献
Fitzmaurice, Jonathan C.; Hector, Andrew L.; Parkin, Ivan P.; Rowley , Adrian T.
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 101, # 1-4 p. 47 - 56