3-(4-溴苯基)异噁唑合成路线 (共 14 条)
反应条件
1: With TsNHOH; potassium carbonate in methanol; water T=20°C; 10 h; 2: With potassium carbonate in methanol; water T=60°C; 4 h; regioselective reaction;
参考文献
Tang, Shibing; He, Jinmei; Sun, Yongquan; He, Liuer; She, Xuegong
Organic Letters, 2009 , vol. 11, # 17 p. 3982 - 3985
反应条件
cesium fluoride in ethanol; acetonitrile 0.0833333 h;
参考文献
US2005/85512 A1, ;
Page/Page column 16 ;
反应条件
sodium azide in dimethyl sulfoxide T=10 - 30°C; 0.333333 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 45, # 2 p. 311 - 317
反应条件
manganese(IV) oxide in chloroform T=20°C; 5 h;
参考文献
Synthesis, , # 1 p. 49 - 52
反应条件
in toluene T=110°C; 0.75 h;
参考文献
Baranski, Andrzej; Shvekhgeimer, Genrikh A.
Polish Journal of Chemistry, 1982 , vol. 56, # 3 p. 459 - 467
反应条件
hydrogenchloride in ethanol 12 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 17, p. 881 - 885
反应条件
pyridine; hydroxylamine hydrochloride in ethanol T=78°C; 16 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 45, # 3 p. 879 - 885
反应条件
1: diethyl ether / 4 h / Heating 2: aq. NaOH / 0.08 h / Heating View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 6, p. 598 - 602
反应条件
1: Br2 / CH2Cl2 / 0.33 h / 0 °C 2: NaN3 / dimethylsulfoxide / 24 h / 20 °C 3: aq. NaOH / dimethylsulfoxide / 92 h / 0 °C 4: 6 percent / MnO2 / CHCl3 / 5 h / 20 °C View Scheme
参考文献
Synthesis, , # 1 p. 49 - 52
反应条件
1: N-chlorosuccinimide / CHCl3 / Ambient temperature 2: 75 percent / triethylamine / acetonitrile / Ambient temperature 3: 25 percent / 37percent hydrochloric acid / ethanol / 12 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 17, p. 881 - 885