N-(2-甲酰基苯基)乙酰胺合成路线 (共 32 条)
反应条件
aluminum oxide Solid phase reaction; cycloaddition; 0.133333 h; microwave irradiation;
参考文献
Sharma, Utpal; Ahmed, Shahadat; Boruah, Romesh C.
Tetrahedron Letters, 2000 , vol. 41, # 18 p. 3493 - 3495
反应条件
1: concentrated alcoholic ammonia 2: chromium trioxide; glacial acetic acid View Scheme
参考文献
Bischler; Lang
Chemische Berichte, 1895 , vol. 28, p. 292
反应条件
aluminum oxide Solid phase reaction; cycloaddition; 0.141667 h; microwave irradiation;
参考文献
Sharma, Utpal; Ahmed, Shahadat; Boruah, Romesh C.
Tetrahedron Letters, 2000 , vol. 41, # 18 p. 3493 - 3495
反应条件
perchloric acid; ethyl N-chlorocarbamate; acetic acid in water T=29.9°C; 10 h; ΔH(excit.), ΔS(excit.), ΔG(excit.); Rate constantKineticsThermodynamic data;
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, , vol. 32, # 1-3 p. 205 - 209
反应条件
1: Cs2CO3 / dimethylformamide / 40 °C 2: Cs2CO3 / dimethylformamide / 60 °C View Scheme
参考文献
Park, Kwanghee Koh; Jung, Jin Young
Heterocycles, 2005 , vol. 65, # 9 p. 2095 - 2105
反应条件
caesium carbonate in N,N-dimethyl-formamide T=60°C; intramolecular Aldol-type condensation;
参考文献
Park, Kwanghee Koh; Jung, Jin Young
Heterocycles, 2005 , vol. 65, # 9 p. 2095 - 2105
反应条件
water; hydroxide in 1,4-dioxane T=30°C; ΔH(excit.), ΔS(excit.); Thermodynamic dataRate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 2 p. 1133 - 1138
反应条件
potassium dihydrogenphosphate; hydroxylamine hydrochloride in ethanol T=20°C; 2 h;
参考文献
Saikia, Anil; Barthakur, Madan G.; Borthakur, Moyurima; Saikia, Chandan J.; Bora, Utpal; Boruah, Romesh C.
Tetrahedron Letters, 2006 , vol. 47, # 1 p. 43 - 46
反应条件
1: alcohol; water; sodium hydroxide; hydroxylamine hydrochloride 2: glacial acetic acid; alcohol; sodium amalgam View Scheme
参考文献
Bischler
Chemische Berichte, 1893 , vol. 26, p. 1901
反应条件
triethylamine in dichloromethane
T=0 - 20°C; 18 h;
参考文献
STERIX LIMITED
Patent: WO2009/66072 A2, 2009 ;
Location in patent: Page/Page column 55; 58 ;
WO 2009/066072 A2