N-(2-甲酰基苯基)乙酰胺合成路线 (共 32 条)
反应条件
1: aq. sodium dodecyl sulfate, HCl / 0.75 h
2: 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / H2O; tetrahydrofuran / 0.5 h
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参考文献
Bonar-Law, Richard P.
Journal of Organic Chemistry, 1996 , vol. 61, # 11 p. 3623 - 3634
反应条件
1: 35 percent / PPh3; Zn / CH2Cl2 / 12 h / 20 °C
2: 52 percent / Pd2(dba)3; dppf; Et3N / toluene / 12 h / 100 °C
3: 100 percent / NaOH / ethanol; H2O / 0.17 h / 70 °C
View Scheme
参考文献
Thielges, Sabine; Meddah, Emilie; Bisseret, Philippe; Eustache, Jacques
Tetrahedron Letters, 2004 , vol. 45, # 5 p. 907 - 910