2,4,6-三(苯基)膦咛合成路线 （共 13 条）
参考文献
Breit, Bernhard; Winde, Roland; Mackewitz, Thomas; Paciello, Rocco; Harms, Klaus
Chemistry - A European Journal, 2001 , vol. 7, # 14 p. 3106 - 3121
反应条件
tris(trimethyl-silyl)-phosphine in acetonitrile
参考文献
DiMauro, Erin F.; Kozlowski, Marisa C.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 439 - 444
反应条件
1: 4 h / 80 °C / |Schlenk technique; |Inert atmosphere 2: tris(trimethyl-silyl)-phosphine / ethylene glycol dimethyl ether / 16 h / 90 °C View Scheme
参考文献
Broeckx, Leen E. E.; Gueven, Sabriye; Heutz, Frank J. L.; Lutz, Martin; Vogt, Dieter; Mueller, Christian
Chemistry - A European Journal, 2013 , vol. 19, # 39 p. 13087 - 13098
反应条件
pyridine; tris (hydroxy methyl)-phosphine
参考文献
Tolmachev,A.I.; Kozlov,E.S.
J. Gen. Chem. USSR (Engl. Transl.), 1967 , vol. 37, p. 1921 - 1922,1826
反应条件
hydrogenchloride; lithium aluminium tetrahydride 1.) methanol, 2 h, reflux; 2.) di-n-butylether, 2 h, reflux; Yield given. Multistep reaction;
参考文献
Dimroth, Karl; Kaletsch, Hans
Chemische Berichte, 1987 , vol. 120, p. 1245 - 1248
反应条件
1: Br2 / CCl4; acetonitrile 2: benzene / Ambient temperature View Scheme
参考文献
Kanter,H. et al.
Chemische Berichte, 1977 , vol. 110, p. 395 - 422
反应条件
mercury(II) diacetate in benzene
参考文献
Dimroth,K.; Staede,W.
Angewandte Chemie, 1968 , vol. 80, p. 966 - 967
反应条件
1: PCl5 / CCl4; acetonitrile / Irradiation 2: benzene View Scheme
参考文献
Kanter,H. et al.
Chemische Berichte, 1977 , vol. 110, p. 395 - 422
反应条件
potassium tert-butylate
参考文献
Maerkl,G.; Merz,A.
Tetrahedron Letters, 1971 , p. 1269 - 1272
反应条件
potassium tert-butylate
参考文献
Maerkl,G.; Merz,A.
Tetrahedron Letters, 1971 , p. 1269 - 1272
