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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-甲氧基苯甲醛
合成路线
（共 720 条）
64-17-5
乙醇
+
135-02-4
2-甲氧基苯甲醛
→
反应条件
64988-06-3
2-(乙氧基甲基)苯甲醚
反应条件
Decaborane T=20°C; reductive etherification; 6.5 h;
参考文献
Lee, Seung Hwan; Park, Yong June; Yoon, Cheol Min
Tetrahedron Letters, 1999 , vol. 40, # 33 p. 6049 - 6050
135-02-4
2-甲氧基苯甲醛
→
反应条件
651331-49-6
反应条件
1.1: 68 percent / methanol / 1.5 h / -10 °C 2.1: 88 percent / xylene / 1 h / Heating 3.1: 99 percent / aq. NaOH / 0.5 h / Heating 4.1: 94 percent / Cu; quinoline / 2 h / Heating 5.1: 85 percent / phosphoryl chloride / 1.5 h / 0 - 40 °C 6.1: NaOH / CH2Cl2 / 0.5 h / 20 °C 6.2: 97 percent / CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
135-02-4
2-甲氧基苯甲醛
→
反应条件
651331-65-6
反应条件
1.1: 68 percent / methanol / 1.5 h / -10 °C 2.1: 88 percent / xylene / 1 h / Heating 3.1: 99 percent / aq. NaOH / 0.5 h / Heating 4.1: 94 percent / Cu; quinoline / 2 h / Heating 5.1: 85 percent / phosphoryl chloride / 1.5 h / 0 - 40 °C 6.1: NaOH / CH2Cl2 / 0.5 h / 20 °C 6.2: 97 percent / CH2Cl2 / 12 h / 20 °C 7.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / 0 °C 7.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0.25 h / 0 °C 7.3: 74 percent / tetrahydrofuran; hexane / 2.5 h / -78 - 0 °C 8.1: 93 percent / H2 / Pd/C / ethanol / 4 h / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
135-02-4
2-甲氧基苯甲醛
→
反应条件
651331-68-9
反应条件
1.1: 68 percent / methanol / 1.5 h / -10 °C 2.1: 88 percent / xylene / 1 h / Heating 3.1: 99 percent / aq. NaOH / 0.5 h / Heating 4.1: 94 percent / Cu; quinoline / 2 h / Heating 5.1: 85 percent / phosphoryl chloride / 1.5 h / 0 - 40 °C 6.1: NaOH / CH2Cl2 / 0.5 h / 20 °C 6.2: 97 percent / CH2Cl2 / 12 h / 20 °C 7.1: n-BuLi; potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C 7.2: 71 percent / tetrahydrofuran; hexane / -78 - 0 °C 8.1: 94 percent / H2 / Pd/C / ethanol / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
135-02-4
2-甲氧基苯甲醛
→
反应条件
651331-69-0
反应条件
1.1: 68 percent / methanol / 1.5 h / -10 °C 2.1: 88 percent / xylene / 1 h / Heating 3.1: 99 percent / aq. NaOH / 0.5 h / Heating 4.1: 94 percent / Cu; quinoline / 2 h / Heating 5.1: 85 percent / phosphoryl chloride / 1.5 h / 0 - 40 °C 6.1: NaOH / CH2Cl2 / 0.5 h / 20 °C 6.2: 97 percent / CH2Cl2 / 12 h / 20 °C 7.1: n-BuLi / tetrahydrofuran; hexane / 0 °C 7.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C 7.3: 45 percent / tetrahydrofuran; hexane / -78 - 0 °C 8.1: 57 percent / H2 / Pd/C / ethanol / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
135-02-4
2-甲氧基苯甲醛
→
反应条件
651331-70-3
反应条件
1.1: 68 percent / methanol / 1.5 h / -10 °C 2.1: 88 percent / xylene / 1 h / Heating 3.1: 99 percent / aq. NaOH / 0.5 h / Heating 4.1: 94 percent / Cu; quinoline / 2 h / Heating 5.1: 85 percent / phosphoryl chloride / 1.5 h / 0 - 40 °C 6.1: NaOH / CH2Cl2 / 0.5 h / 20 °C 6.2: 97 percent / CH2Cl2 / 12 h / 20 °C 7.1: n-BuLi / tetrahydrofuran; hexane / 0 °C 7.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C 7.3: 69 percent / tetrahydrofuran; hexane / -78 - 0 °C 8.1: 47 percent / H2 / Pd/C / ethanol / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
135-02-4
2-甲氧基苯甲醛
→
反应条件
651331-71-4
反应条件
1.1: 68 percent / methanol / 1.5 h / -10 °C 2.1: 88 percent / xylene / 1 h / Heating 3.1: 99 percent / aq. NaOH / 0.5 h / Heating 4.1: 94 percent / Cu; quinoline / 2 h / Heating 5.1: 85 percent / phosphoryl chloride / 1.5 h / 0 - 40 °C 6.1: NaOH / CH2Cl2 / 0.5 h / 20 °C 6.2: 97 percent / CH2Cl2 / 12 h / 20 °C 7.1: n-BuLi / tetrahydrofuran; hexane / 0 °C 7.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C 7.3: 68 percent / tetrahydrofuran; hexane / -78 - 0 °C 8.1: 50 percent / H2 / Pd/C / ethanol / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
68536-04-9
+
135-02-4
2-甲氧基苯甲醛
→
反应条件
69790-18-7
N,N'-二(2-甲氧基苄基氨基己基)胱胺
反应条件
(i), (ii) NaBH4; Multistep reaction;
参考文献
Melchiorre,C. et al.
Journal of Medicinal Chemistry, 1978 , vol. 21, p. 1126 - 1132
135-02-4
2-甲氧基苯甲醛
→
反应条件
70311-27-2
乙基3-(2-甲氧基苯基)丙酸酯
反应条件
1: 1) piperidine, 2) conc. H2SO4 / 1) pyridine 2: hydrogen / 5percent Pd/C / ethanol View Scheme
参考文献
Mimori, Seisuke; Okuma, Yasunobu; Kaneko, Masayuki; Kawada, Koichi; Nomura, Yasuyuki; Murakami, Yasuoki; Hamana, Hiroshi
Chemistry Letters, 2013 , vol. 42, # 9 p. 1051 - 1052
135-02-4
2-甲氧基苯甲醛
→
反应条件
709-16-0
L-2-羟基苯丙氨酸
反应条件
1: acetic acid anhydride; sodium acetate / 140 °C 2: hydriodic acid; red phosphorus View Scheme
参考文献
Dickinson; Marshall
Journal of the Chemical Society, 1929 , p. 1496
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