2,2'-二苯甲酰氨基二苯二硫合成路线 (共 12 条)
反应条件
triethylamine in tetrahydrofuran T=20°C; Acylation;
参考文献
Ueno, Takafumi; Inohara, Masahiro; Ueyama, Norikazu; Nakamura, Akira
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 5 p. 1077 - 1083
反应条件
1: 2-amino-benzenethiol With 4-methoxytrityl resin chloride; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 2: benzoic acid With diisopropyl-carbodiimide in N,N-dimethyl-formamide T=20°C; 3 h; 3: With triethylsilane; trifluoroacetic acid in dichloromethane Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 42, # 11 p. 2201 - 2204
反应条件
1: air; diluted ammonia 2: 100 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 46, p. 1310
参考文献
Journal of the Chemical Society, , p. 483 - 486
反应条件
1: hydrazine hydrate; alcohol 2: acetic acid ester View Scheme
参考文献
Chemische Berichte, , vol. 45, p. 133
反应条件
1: Na2S2 2: hydrazine hydrate; alcohol 3: acetic acid ester View Scheme
参考文献
Chemische Berichte, , vol. 45, p. 133
反应条件
1: sulfur 2: alkali View Scheme
参考文献
Journal of the Chemical Society, , p. 2320
反应条件
1: o-bensoylaminobenzene thiolate disulfide With sodium tetrahydroborate in ethanol T=0 - 20°C; 0.5 h; 2: benzoyl chloride With potassium carbonate in ethanol T=0 - 20°C; pH=9 - 10; Further stages.;
参考文献
Villalobos, Janette M.; Srogl, Jiri; Liebeskind, Lanny S.
Journal of the American Chemical Society, 2007 , vol. 129, # 51 p. 15734 - 15735
反应条件
hydrogenchloride; tin
参考文献
Journal of the American Chemical Society, , vol. 46, p. 1310
参考文献
Journal of the American Chemical Society, , vol. 46, p. 1310