1-[4-(4-硝基苯基)苯基]乙酮合成路线 （共 22 条）
反应条件
1: NaBrO 2: aqueous <NH4>2S View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 2479,2480
参考文献
Du Pont de Nemours and Co.
Patent: US2742499 , 1952 ;
反应条件
1: aq. NaOBr / dioxane 2: (i) SOCl2, (ii) /BRN= 1098229/ View Scheme
参考文献
Byron,D.J. et al.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 840 - 845
反应条件
1: aq. NaOBr / dioxane 2: (i) SOCl2, (ii) /BRN= 1098229/ 3: Fe, aq. HCl / methanol View Scheme
参考文献
Byron,D.J. et al.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 840 - 845
反应条件
sodium azide; sulfuric acid; acetic acid Hydrolysieren des Reaktionsprodukts;
参考文献
Szmant; McIntosh
Journal of the American Chemical Society, 1950 , vol. 72, p. 4835
反应条件
hydrogenchloride; SnCl3(1-) in ethanol 1 h; Heating;
参考文献
Gogrichiani, E. O.; Chikvaidze, I. Sh.; Dzhibladze, L. I.; Tsotadze, M. B.; Samsoniya, Sh. A.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1994 , vol. 30, # 10 p. 1170 - 1173
Chimia, 1994 , # 10 p. 1351 - 1354
反应条件
sodium carbonate; palladium on activated charcoal in ethanol
T=20°C; Suzuki-Miyaura cross-coupling; 19 h;
参考文献
Monguchi, Yasunari; Fujita, Yuki; Hashimoto, Shota; Ina, Mariko; Takahashi, Tohru; Ito, Ryo; Nozaki, Kei; Maegawa, Tomohiro; Sajiki, Hironao
Tetrahedron, 2011 , vol. 67, # 45 p. 8628 - 8634
反应条件
glucosamine-based dicyclohexylarylphosphine; sodium carbonate; palladium diacetate in ethanol; water; toluene
T=80°C; Suzuki-Miyaura cross coupling reaction;
参考文献
Konovets, Anzhelika; Penciu, Alexandra; Framery, Eric; Percina, Nathalie; Goux-Henry, Catherine; Sinou, Denis
Tetrahedron Letters, 2005 , vol. 46, # 18 p. 3205 - 3208
反应条件
Ti2CO3; tetrakis(triphenylphosphine) palladium(0) in benzene
T=80°C; 6 h;
参考文献
Sato, Makoto; Miyaura, Norio; Suzuki, Akira
Chemistry Letters, 1989 , p. 1405 - 1408
反应条件
potassium carbonate in ethanol
T=80°C; Suzuki-Miyaura coupling; 12 h; Inert atmosphere;
参考文献
Hoshiya, Naoyuki; Shimoda, Masahiko; Yoshikawa, Hideki; Yamashita, Yoshiyuki; Shuto, Satoshi; Arisawa, Mitsuhiro
Journal of the American Chemical Society, 2010 , vol. 132, # 21 p. 7270 - 7272
