1-[4-(4-硝基苯基)苯基]乙酮合成路线 （共 22 条）
反应条件
{C6H3[NHP(piperidinyl)2]2Pd(Cl)}; potassium carbonate in 1,4-dioxane; water; butan-1-ol
T=100°C; Suzuki-Miyaura reaction; 3 h;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 6 p. 1075 - 1080
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in N,N-dimethyl-formamide
T=80°C; 18 h;
参考文献
Zhu, Lei; Duquette, Jason; Zhang, Mingbao
Journal of Organic Chemistry, 2003 , vol. 68, # 9 p. 3729 - 3732
反应条件
carbon disulfide; aluminium trichloride
T=45 - 50°C;
参考文献
Grieve; Hey
Journal of the Chemical Society, 1933 , p. 968,971
反应条件
1: palladium(II) acetate; potassium acetate / dimethylformamide / 18 h / 80 °C
2: Cs2CO3; Pd(PPh3)4 / dimethylformamide / 18 h / 80 °C
View Scheme
参考文献
Zhu, Lei; Duquette, Jason; Zhang, Mingbao
Journal of Organic Chemistry, 2003 , vol. 68, # 9 p. 3729 - 3732
反应条件
Br(1-)*C24H31BrN5O6Pd(1+); sodium hydroxide in water
T=160°C; Hiyama coupling; 2 h; Sealed tube;
参考文献
Ines, Blanca; Moure, Maria Jesus; SanMartin, Raul; Herrero, Maria Teresa; Moreno, Isabel; Dominguez, Esther
Arkivoc, 2011 , vol. 2011, # 3 p. 191 - 199
反应条件
aluminium trichloride
参考文献
Tsuno,Y. et al.
Bulletin of the Chemical Society of Japan, 1978 , vol. 51, p. 596 - 600
反应条件
nitric acid
T=-5 - 0°C;
参考文献
Grieve; Hey
Journal of the Chemical Society, 1933 , p. 968,971
参考文献
Runti
Annali di Chimica (Rome, Italy), 1954 , vol. 44, p. 489,492
反应条件
in 1,4-dioxane; water
T=30°C; Equilibrium constant;
参考文献
Ananthakrishnanadar, P.; Kannan, N.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 749 - 750
反应条件
sodium ethanolate
T=20°C;
参考文献
Dilthey et al.
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2> 124, p. 123
