2-溴-4-苯基乙酰苯合成路线 （共 108 条）
反应条件
potassium hydroxide; 18-crown-6 ether in acetonitrile
2 h; Yield given;
参考文献
Cane, David E.; Hasler, Heinz; Taylor, Paul B.; Liang, Tzyy-Chyau
Tetrahedron, 1983 , vol. 39, # 21 p. 3449 - 3456
反应条件
(i) CrO3, H2SO4, aq. NaOH, AgO, (ii) /BRN= 513838/, EtOH; Multistep reaction;
参考文献
Bottini,A.T.; Olsen,R.E.
Journal of the American Chemical Society, 1962 , vol. 84, p. 195 - 199
反应条件
(i) aq. KOH, (ii) KMnO4, (iii) /BRN= 513838/, aq. KOH; Multistep reaction;
参考文献
Schulze,K. et al.
Tetrahedron, 1975 , vol. 31, p. 1455 - 1459
参考文献
Wrede; Rothhaas
Chemische Berichte, 1934 , vol. 67, p. 739
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1934 , vol. 226, p. 95,97,102
Full Text Show Details
Drake; Bronitsky
Journal of the American Chemical Society, 1930 , vol. 52, p. 3715,3716, 3719
反应条件
1: methanol
2: aq. H2SO4 / methanol
3: 2,3,5-triphenyl-tetrazolium chloride, <PhCH2NMe3>OH / methanol; CH2Cl2
View Scheme
参考文献
Moehrle; Schittenhelm
Archiv der Pharmazie, 1972 , vol. 305, # 4 p. 309 - 314
参考文献
Kornblum et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 6562
反应条件
in chloroform
72 h; Ambient temperature;
参考文献
Lhotak, Pavel; Kurfuerst, Antonin
Collection of Czechoslovak Chemical Communications, 1993 , vol. 58, # 11 p. 2720 - 2728
反应条件
sodium carbonate; 1-butylpyridinium tetrafluoroborate
T=20°C; Chichibabin cyclocondensation; 4 h;
参考文献
Xu, Danqian; Liu, Baoyou; Zheng, Mei
Journal of Chemical Research - Part S, 2003 , # 10 p. 645 - 647
反应条件
in 1,4-dioxane
T=65°C; 1 h;
参考文献
Floyd, M. Brawner; Du, Mila T.; Fabio, Paul F.; Jacob, Linda A.; Johnson, Bernard D.
Journal of Organic Chemistry, 1985 , vol. 50, # 25 p. 5022 - 5027
反应条件
1.1: tellurium powder / dimethylsulfoxide / 1 h / Heating
1.2: 59 percent / dimethylsulfoxide / 2 h / 20 °C
2.1: NaOH in EtOH; O2 / 0.83 h / 40 °C
2.2: 76 percent / NaOH in EtOH / 1 h / Heating
3.1: 74 percent / activated copper / dioxane / 3 h / Heating
View Scheme
参考文献
Al-Rubaie, Ali Z.; Yousif, Lina Z.; Al-Ba'aj, Ammar K.
Journal of Organometallic Chemistry, 2003 , vol. 673, # 1-2 p. 40 - 46
