2-溴-4-苯基乙酰苯合成路线 （共 108 条）
反应条件
1: 2-acetyl-3,3-bis-ethylsulfanyl-N-o-tolyl-acrylamide With sodium hydroxide in ethanol T=25°C; 0.833333 h; 2: ω-bromo-p-phenyl-acetophenone in ethanol T=25°C;
参考文献
Chinese Journal of Chemistry, , vol. 30, # 2 p. 367 - 371
反应条件
1: 2-[bis(benzylthio)methylene]-3-oxo-N-o-tolylbutanamide With sodium hydroxide in ethanol T=25°C; 0.833333 h; 2: ω-bromo-p-phenyl-acetophenone in ethanol T=25°C;
参考文献
Chinese Journal of Chemistry, , vol. 30, # 2 p. 367 - 371
反应条件
1: NaN3 / ethanol; acetic acid; H2O / cooling 2: 1 percent / toluene / Photolysis View Scheme
参考文献
Singh, Pradeep N. D.; Mandel, Sarah M.; Robinson, Rachel M.; Zhu, Zhendong; Franz, Roberto; Ault, Bruce S.; Gudmundsdottir, Anna D.
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 7951 - 7960
反应条件
in ethanol; water T=20°C; Substitution; 2 h;
参考文献
MERCK and CO., INC.
Patent: WO2005/44785 A1, 2005 ;
Location in patent: Page/Page column 95-96 ;
WO 2005/044785 A1
反应条件
hydroxymethanesulfinic acid sodium salt; potassium hydrogencarbonate in water; N,N-dimethyl-formamide T=80°C; 20 h;
参考文献
Journal of Organic Chemistry, , vol. 53, # 24 p. 5750 - 5756
反应条件
sodium ditelluride; copper dichloride in tetrahydrofuran; N,N-dimethyl-formamide T=-40°C; 2 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 6 p. 2114 - 2116
反应条件
trimethylsilyl iodide in chloroform Ambient temperatureor reflux;
参考文献
Ho, Tse-Lok
Synthetic Communications, 1981 , vol. 11, # 2 p. 101 - 104
反应条件
sulfur dioxide; hydroxymethanesulfinic acid sodium salt in N,N-dimethyl-formamide 18 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 53, # 24 p. 5750 - 5756
反应条件
T=15°C; electrochemical reduction; anode: platinum, cathode: mercury pool;
参考文献
Barba, Fructuoso; Fuente, Jose Luis de la
Tetrahedron Letters, 1992 , vol. 33, # 27 p. 3911 - 3914
反应条件
N,N-dimethyl-aniline in tetrahydrofuran 18 h; Inert atmosphereReflux; ConcentrationReagent/catalyst;
参考文献
Organic Letters, , vol. 15, # 22 p. 5898 - 5901
