2-溴-4-苯基乙酰苯合成路线 （共 108 条）
反应条件
sulfur dioxide; hydroxymethanesulfinic acid sodium salt in N,N-dimethyl-formamide 18 h; Ambient temperature;
参考文献
Jarvis, William F.; Hoey, Michael D.; Finocchio, Alfred L.; Dittmer, Donald C.
Journal of Organic Chemistry, 1988 , vol. 53, # 24 p. 5750 - 5756
反应条件
1: H2O; methanol 2: 96 percent / dimethylformamide / 20 °C / electrolysis; anode: platinum, cathode: mercury pool; lithium perchlorate, potential of -1V (vs saturated calomel electrode) 3: 77 percent / aq. 15percent HCl, HgCl2 / 6 h / Heating View Scheme
参考文献
Barba, Fructuoso; Velasco, M. Desamparados; Guirado, Antonio
Synthesis, 1984 , # 7 p. 593 - 595
反应条件
β-cyclodextrin in methanol; water T=70°C; 2.3 h;
参考文献
Tetrahedron Letters, , vol. 50, # 44 p. 6025 - 6028
反应条件
potassium formiate; sodium hydrogencarbonate in ethanol
T=40°C;
参考文献
Miyazaki, Yasushi; Matsunaga, Shinichiro; Tang, Jun; Maeda, Yutaka; Nakano, Masato; Philippe, Rocher J.; Shibahara, Megumi; Liu, Wei; Sato, Hideyuki; Wang, Liping; Nolte, Robert T.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 9 p. 2203 - 2207
反应条件
hydrogenchloride; ethanol
参考文献
Snell; McElvain
Journal of the American Chemical Society, 1933 , vol. 55, p. 416,427
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Jansen
Journal of Biological Chemistry, 1948 , vol. 176, p. 662
反应条件
in ethanol
T=70°C; 18 h;
参考文献
Buu-Hoi,N.P. et al.
Bulletin de la Societe Chimique de France, 1966 , p. 1277 - 1279
反应条件
chloroform; 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane
Behandeln des Reaktionsprodukts mit wss.-aethanol. Salzsaeure;
参考文献
Ying-lin, Han; Hong-ven, Hu
Tetrahedron Letters, 1989 , vol. 30, # 39 p. 5285 - 5286
反应条件
hydrogenchloride
1a) EtOH, RT, 2h, 1b) 50 deg C, 30 min, 2) 30 min, reflux; Yield given. Multistep reaction;
参考文献
Ying-lin, Han; Hong-ven, Hu
Tetrahedron Letters, 1989 , vol. 30, # 39 p. 5285 - 5286
参考文献
Tewari, R. S.; Dubey, A. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 2 p. 153 - 154
反应条件
lithium hydride in tetrahydrofuran
T=-5 - 0°C; 12 h;
参考文献
Lin, Chun Min; Wong, Fung Fuh; Huang, Jiann-Jyh; Yeh, Mou-Yung
Heterocycles, 2006 , vol. 68, # 7 p. 1359 - 1370
