1,2,4-三甲氧基苯合成路线 （共 122 条）
反应条件
trimethylsilyl trifluoromethanesulfonate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane
T=-78°C;
参考文献
Morimoto, Koji; Sakamoto, Kazuma; Ohnishi, Yusuke; Miyamoto, Takeshi; Ito, Motoki; Dohi, Toshifumi; Kita, Yasuyuki
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 8726 - 8731
反应条件
trimethylsilyl trifluoromethanesulfonate in hexafluoroisopropyl alcohol
T=20°C; 3 h; Inert atmosphere;
参考文献
Dohi, Toshifumi; Ito, Motoki; Yamaoka, Nobutaka; Morimoto, Koji; Fujioka, Hiromichi; Kita, Yasuyuki
Angewandte Chemie - International Edition, 2010 , vol. 49, # 19 p. 3334 - 3337
反应条件
Et3NCH3 O3SOCH3; hexafluoroisopropyl alcohol
T=50°C; Electrolysis;
参考文献
Kirste, Axel; Schnakenburg, Gregor; Stecker, Florian; Fischer, Andreas; Waldvogel, Siegfried R.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 5 p. 971 - 975
反应条件
Et3NCH3 O3SOCH3; hexafluoroisopropyl alcohol
T=50°C; Electrolysis;
参考文献
Kirste, Axel; Schnakenburg, Gregor; Stecker, Florian; Fischer, Andreas; Waldvogel, Siegfried R.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 5 p. 971 - 975
反应条件
sulfuric acid; acetone
bei der Elektrolyse an Blei-Anoden;
参考文献
Erdtman
Proceedings of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences, 1934 , vol. 143, p. 196,197
Chem. Zentralbl., 1934 , vol. 105, # I p. 3054
反应条件
nitrogen(IV) oxide in dichloromethane
T=-78°C; 2 h; UV spectra; Product distribution;
参考文献
Rathore; Bosch; Kochi
Tetrahedron, 1994 , vol. 50, # 23 p. 6727 - 6758
反应条件
aluminium trichloride; benzene
参考文献
Govindachari et al.
Journal of the Chemical Society, 1958 , p. 912
参考文献
Erdtman
Proceedings of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences, 1934 , vol. 143, p. 196,197
Chem. Zentralbl., 1934 , vol. 105, # I p. 3054
参考文献
Erdtman
Proceedings of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences, 1934 , vol. 143, p. 196,197
Chem. Zentralbl., 1934 , vol. 105, # I p. 3054
反应条件
aluminium trichloride in dichloromethane
T=10°C; 1 h;
参考文献
Hoegberg, Thomas; Bengtsson, Stefan; Paulis, Tomas de; Johansson, Lars; Stroem, Peter; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 4 p. 1155 - 1163
