反应条件
1: 1.) Mg, 2.) Li2CuCl4 / 1.) ether, THF, 2.) THF, -78 to -55 deg C, 1 h
2: aq. concd. HCl / methanol / 48 h / 20 °C
3: 1.) HBr, 2.) KOH / 1.) glacial acetic acid, 0 deg C, 5 min, 2.) methanol, 15 min
View Scheme
参考文献
Hoeyer, Thomas; Kjaer, Anders; Lykkesfeldt, Jens
Collection of Czechoslovak Chemical Communications, 1991 , vol. 56, # 5 p. 1042 - 1051
