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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-氯-6-碘哒嗪
合成路线
（共 21 条）
141-30-0
3,6-二氯哒嗪
→
反应条件
135034-10-5
3-氯-6-碘哒嗪
反应条件
hydrogen iodide; sodium iodide in hexane T=40°C; 4 h; Inert atmosphere;
参考文献
US2010/4443 A1, ;
Page/Page column 34 ;
17973-86-3
3,6-二溴哒嗪
→
反应条件
135034-10-5
3-氯-6-碘哒嗪
反应条件
1: With hydrogen iodide; sodium iodide in water T=40°C; 18 h; 2: With sodium hydroxide in water T=20°C; pH=> 12;
参考文献
WO2007/22937 A1, ;
Page/Page column 26 ;
WO 2007/022937 A1
1120-95-2
3-氯哒嗪
→
反应条件
135034-10-5
3-氯-6-碘哒嗪
反应条件
potassium iodide in hydrogen iodide T=40°C; 24 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 8 p. 1896 - 1900
5720-07-0
4-甲氧基苯硼酸
+
135034-10-5
3-氯-6-碘哒嗪
→
反应条件
2166-07-6
+
58059-31-7
3-氯-6-(4-甲氧苯基)哒嗪
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in 1,4-dioxane Suzuki Coupling; HeatingInert atmosphere; chemoselective reaction;
参考文献
European Journal of Organic Chemistry, , # 1 p. 117 - 124
33397-21-6
+
135034-10-5
3-氯-6-碘哒嗪
→
反应条件
58059-31-7
3-氯-6-(4-甲氧苯基)哒嗪
反应条件
palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 4 h; Inert atmosphere; Catalytic behavior; Reagent/catalyst; chemoselective reaction;
参考文献
Urgin, Karene; Aube, Christophe; Pipelier, Muriel; Blot, Virginie; Thobie-Gautier, Christine; Sengmany, Stephane; Lebreton, Jacques; Leonel, Eric; Dubreuil, Didier; Condon, Sylvie
European Journal of Organic Chemistry, 2013 , # 1 p. 117 - 124
544-92-3
氰化亚铜
+
135034-10-5
3-氯-6-碘哒嗪
→
反应条件
35857-89-7
3-氯-6-氰基哒嗪
反应条件
in acetonitrile T=160°C; 0.5 h; Microwave irradiation;
参考文献
JANSSEN PHARMACEUTICA N.V.
Patent: WO2008/68277 A1, 2008 ;
Location in patent: Page/Page column 18-19 ;
WO 2008/068277 A1
→
反应条件
35857-89-7
3-氯-6-氰基哒嗪
反应条件
in acetonitrile T=160°C; 0.5 h; Microwave irradiation;
参考文献
NOVARTIS AG; HEBACH, Christina; KALLEN, Joerg; NOZULAK, Joachim; TINTELNOT-BLOMLEY, Marina; WIDLER, Leo
Patent: WO2013/80120 A1, 2013 ;
Location in patent: Page/Page column 68 ;
5142-75-6
三对甲苯基铋
+
135034-10-5
3-氯-6-碘哒嗪
→
反应条件
2165-06-2
3-氯-6-邻-甲苯哒嗪
反应条件
palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 4 h; Inert atmosphere; chemoselective reaction;
参考文献
Urgin, Karene; Aube, Christophe; Pipelier, Muriel; Blot, Virginie; Thobie-Gautier, Christine; Sengmany, Stephane; Lebreton, Jacques; Leonel, Eric; Dubreuil, Didier; Condon, Sylvie
European Journal of Organic Chemistry, 2013 , # 1 p. 117 - 124
26919-48-2
+
135034-10-5
3-氯-6-碘哒嗪
→
反应条件
66549-34-6
3-氯-6-(3-甲基苯基)-哒嗪
反应条件
palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 4 h; Inert atmosphere; chemoselective reaction;
参考文献
Urgin, Karene; Aube, Christophe; Pipelier, Muriel; Blot, Virginie; Thobie-Gautier, Christine; Sengmany, Stephane; Lebreton, Jacques; Leonel, Eric; Dubreuil, Didier; Condon, Sylvie
European Journal of Organic Chemistry, 2013 , # 1 p. 117 - 124
→
反应条件
258506-68-2
3-氯-6-三氟甲基哒嗪
反应条件
potassium fluoride; copper(l) iodide in DMF (N,N-dimethyl-formamide) T=120°C; 5 h;
参考文献
Kalypsys, Inc.
Patent: US2005/234046 A1, 2005 ;
Location in patent: Page/Page column 66 ;
US 20050234046 A1
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