N-(对甲苯磺酰)-L-苯丙氨酸合成路线 (共 22 条)
反应条件
sodium hydroxide in diethyl ether; water T=0°C; 4 h;
参考文献
Saravanan; Sadhukhan, Arghya; Khan, Noor-Ul H.; Kureshy, Rukhsana I.; Abdi, Sayed H. R.; Bajaj, Hari C.
Journal of Organic Chemistry, 2012 , vol. 77, # 9 p. 4375 - 4384
反应条件
1: phenyllithium With copper (I) cyanide in tetrahydrofuran; anhydrous butyl ether T=-78 - 20°C; 0.5 h; 2: (2S)-N-para-toluenesulfonylaziridine-2-carboxylic acid in tetrahydrofuran; anhydrous butyl ether T=-78 - 20°C; 21 h; Further stages.;
参考文献
Beresford, Kenneth J. M.; Church, Nicola J.; Young, Douglas W.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 15 p. 2888 - 2897
反应条件
cyclohexa-1,4-diene; palladium on activated charcoal in methanol 6 h; Heating;
参考文献
Tetrahedron, , vol. 62, # 51 p. 11955 - 11962
反应条件
sodium hydroxide in 1,4-dioxane T=0°C; 9 h;
参考文献
Piloto, Ana M.; Rovira, Daniel; Costa, Susana P.G.; Goncalves, M. Sameiro T.
Tetrahedron, 2006 , vol. 62, # 51 p. 11955 - 11962
反应条件
pyridine in tetrahydrofuran T=10°C; 0.25 h;
参考文献
Synthetic Communications, , vol. 21, # 6 p. 833 - 839
参考文献
Church, Nicola J.; Young, Douglas W.
Tetrahedron Letters, 1995 , vol. 36, # 1 p. 151 - 154
反应条件
Tris-HCl buffer; water; dimethyl sulfoxide; calcium chloride; chymotrypsin T=25°C;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 32, # 1 p. 336 - 339
反应条件
N,N'-dimethyl-N,N'-propyleneurea; samarium diiodide in tetrahydrofuran 11 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Vedejs, Edwin; Lin, Shouzhong
Journal of Organic Chemistry, 1994 , vol. 59, # 7 p. 1602 - 1603
反应条件
sulfuric acid in chlorobenzene T=60 - 70°C; 8 h;
参考文献
Seong, Mi Ra; Song, Hyun Nam; Kim, Jae Nyoung
Tetrahedron Letters, 1998 , vol. 39, # 39 p. 7101 - 7104
反应条件
sulfuric acid T=60 - 70°C; 8 h;
参考文献
Tetrahedron Letters, , vol. 39, # 39 p. 7101 - 7104