2-甲基-6-硝基苯甲酸合成路线 （共 34 条）
反应条件
phosphorus pentachloride in cyclohexane
1 h; Heating;
参考文献
Peet, Norton P.; Baugh, Larry E.; Sunder, Shyam; Lewis, Jon E.; Matthews, Emily H.; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 11 p. 2403 - 2409
反应条件
1: 55 percent / FeSO4*7H2O, 32 percent aq. ammonia / H2O / 0.08 h / Heating
2: 0.25 h / 235 °C
3: 75 percent / PCl5, POCl3 / 2 h / Heating
View Scheme
参考文献
Mitidieri-Costanza, Angela; Sleiter, Giancarlo
Journal fuer Praktische Chemie (Leipzig), 1985 , vol. 327, # 5 p. 865 - 867
反应条件
sodium tetrahydroborate; boron trifluoride dimethyl etherate in tetrahydrofuran
T=0 - 20°C;
参考文献
McAllister, Laura A.; Bechle, Bruce M.; Dounay, Amy B.; Evrard, Edelweiss; Gan, Xinmin; Ghosh, Somraj; Kim, Ji-Young; Parikh, Vinod D.; Tuttle, Jamison B.; Verhoest, Patrick R.
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3484 - 3497
反应条件
hydrogenchloride in tetrahydrofuran
参考文献
ATandT Bell Laboratories
Patent: US5200544 A1, 1993 ;
