3 - 氯丙基二甲基乙氧基硅烷合成路线 （共 11 条）
反应条件
5 h; Heating / reflux; Product distribution / selectivity;
参考文献
Ramdani, Kamel; Vogin, Bernard; Guennount, Nathalie
Patent: US2005/245755 A1, 2005 ;
Location in patent: Page/Page column 8 ;
反应条件
hydrogenchloride; chlorobis(cyclooctene)rhodium(I) dimer in 1,4-dioxane; chloroform T=20°C; 2 h;
参考文献
Park, Jung-Woo; Jun, Chul-Ho
Organic Letters, 2007 , vol. 9, # 20 p. 4073 - 4076
反应条件
1: ethoxydimethylsilane With ruthenium trichloride in toluene T=20 - 80°C; Under N2 atmosphere; 2: 3-chloroprop-1-ene in toluene T=80°C; 1 h; Under N2 atmosphere;
参考文献
Westmeyer, Mark D.; Bowman, Mark P.; Schilling JR., Curtis L.; Powell, Michael R.
Patent: US2004/92759 A1, 2004 ;
Location in patent: Page 6 ;
参考文献
Guennouni, Nathalie; Mignani, Gerard; Pevere, Virginie
Patent: US2005/70731 A1, 2005 ;
Location in patent: Page/Page column 9; 10 ;
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium T=-78 - 40°C; pressure tight tube; Product distribution / selectivity;
参考文献
DOW CORNING CORPORATION
Patent: WO2009/111095 A1, 2009 ;
Location in patent: Page/Page column 13-14 ;
反应条件
[Ir(acetylacetonate)(1,5-cyclooctadiene)] T=-78 - 60°C; pressure tight tube; Product distribution / selectivity;
参考文献
DOW CORNING CORPORATION
Patent: WO2009/111095 A1, 2009 ;
Location in patent: Page/Page column 12-13 ;
反应条件
in tetrahydrofuran T=70°C; 4 h; Product distribution / selectivity;
参考文献
Vidal, Thierry
Patent: US2010/185005 A1, 2010 ;
Location in patent: Page/Page column 8 ;
反应条件
1: With sodium hydroxide in methanol; water T=20°C; 1.5 h; 2: With potassium dihydrogenphosphate T=20°C; pH=7;
参考文献
JP2004/520272 A, ;
Page/Page column 14-15 ;
反应条件
1: With sodium hydroxide in methanol; water T=20°C; 1.5 h; 2: With potassium dihydrogenphosphate T=20°C; pH=7;
参考文献
JP2004/520272 A, ;
Page/Page column 14-15 ;
反应条件
1: NH3 2: aqueous KOH View Scheme
参考文献
Saam; Speier
Journal of Organic Chemistry, 1959 , vol. 24, p. 119
