反应条件
1: DIBALH / CH2Cl2 / 5 h / -80 °C
2: citric acid / methanol / 3 h / Ambient temperature
3: pyridine, DMAP / 5 h / Ambient temperature
4: 70percent aq. AcOH / 6 h / 60 °C
5: NaIO4 / RuO2*H2O / acetone; H2O / 3 h / Ambient temperature
6: diethyl ether
View Scheme
参考文献
Casiraghi, Giovanni; Colombo, Lino; Rassu, Gloria; Spanu, Pietro
Journal of Organic Chemistry, 1991 , vol. 56, # 23 p. 6523 - 6527
