苯基硫代氨基甲酸S-甲酯合成路线 （共 25 条）
参考文献
Will
Chemische Berichte, 1882 , vol. 15, p. 342
反应条件
(i) AgNO3, MeCN, (ii) /BRN= 605269/; Multistep reaction;
参考文献
Ferris,A.F.; Schutz,B.A.
Journal of Organic Chemistry, 1963 , vol. 28, p. 71 - 74
参考文献
Will
Chemische Berichte, 1882 , vol. 15, p. 342
参考文献
Will
Chemische Berichte, 1882 , vol. 15, p. 342
反应条件
1: carbon monoxide; aniline With sulfur; 1,8-diazabicyclo[5.4.0]undec-7-ene in dimethyl sulfoxide
T=20°C; P=760 Torr; 5 h;
2: methyl iodide in dimethyl sulfoxide
T=20°C; 1 h;
参考文献
Mizuno, Takumi; Iwai, Toshiyuki; Ishino, Yoshio
Tetrahedron, 2005 , vol. 61, # 38 p. 9157 - 9163
反应条件
1: dimethyl-disulfide With aluminium trichloride; zinc in water; acetonitrile
T=65°C; 1.5 h;
2: phenyl isocyanate in water; acetonitrile
T=65°C; 0.5 h;
参考文献
Movassagh, Barahman; Zakinezhad, Yousef
Chemistry Letters, 2005 , vol. 34, # 10 p. 1330 - 1331
反应条件
1: phenyl isocyanate With LiAlHSH in tetrahydrofuran
T=20°C; 1 h;
2: methyl iodide in tetrahydrofuran
T=20°C; 3 h;
参考文献
Koketsu, Mamoru; Kobayashi, Chikashi; Ishihara, Hideharu
Heteroatom Chemistry, 2003 , vol. 14, # 4 p. 374 - 378
反应条件
triethyl(methyl)ammonium S-methyl carbonodithioate
T=45°C; neat (no solvent);
参考文献
Degani, Iacopo; Fochi, Rita; Magistris, Claudio
Synthesis, 2010 , # 7 art. no. Z24809SS, p. 1113 - 1122
反应条件
1: sulfur / tetrahydrofuran / 18 h / 20 °C / 760 Torr
2: tetrahydrofuran / 2 h / 20 °C
View Scheme
参考文献
Mizuno, Takumi; Takahashi, Junko; Ogawa, Akiya
Tetrahedron, 2003 , vol. 59, # 8 p. 1327 - 1331
反应条件
triethylamine in methanol
T=20°C; 0.5 h;
参考文献
Doukara, Abdallah Larbi; Mehdid, Mohammed Amine; Djafri, Ayada; Andreoli, Federico; Vanthuyne, Nicolas; Roussel, Christian
Tetrahedron, 2010 , vol. 66, # 10 p. 1852 - 1858
