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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1350927-23-9
合成路线
(共 6 条)
90-14-2
1-碘萘
+
1350927-23-9
→
反应条件
604-53-5
1,1'-联萘
+
605-02-7
1-苯基萘
反应条件
1: triallyl(phenyl)germane With antimony(V) fluoride on graphite in toluene Inert atmosphereHeating; 2: monoiodonaphthalene With tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran; water; toluene 18 h; Inert atmosphereHeating; chemoselective reaction;
参考文献
Chemistry Letters, , vol. 40, # 9 p. 967 - 969
90-11-9
1-溴代萘
+
1350927-23-9
→
反应条件
605-02-7
1-苯基萘
反应条件
1: triallyl(phenyl)germane With antimony(V) fluoride on graphite in toluene Inert atmosphereHeating; 2: 1-Bromonaphthalene With tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran; water; toluene 18 h; Inert atmosphereHeating; chemoselective reaction;
参考文献
Pitteloud, Jean-Philippe; Liang, Yong; Wnuk, Stanislaw F.
Chemistry Letters, 2011 , vol. 40, # 9 p. 967 - 969
90-14-2
1-碘萘
+
1350927-23-9
→
反应条件
604-53-5
1,1'-联萘
+
605-02-7
1-苯基萘
反应条件
1: triallyl(phenyl)germane With antimony(V) fluoride on graphite in toluene Inert atmosphereHeating; 2: monoiodonaphthalene With tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran; water; toluene 18 h; Inert atmosphereHeating; chemoselective reaction;
参考文献
Chemistry Letters, , vol. 40, # 9 p. 967 - 969
90-14-2
1-碘萘
+
1350927-23-9
→
反应条件
1855-47-6
2-异丙苯基萘
+
2489-86-3
反应条件
1: With sodium hydroxide in 1,4-dioxane T=20°C; 0.25 h; 2: With palladium diacetate T=95°C; 18 h; chemoselective reaction;
参考文献
Pitteloud, Jean-Philippe; Liang, Yong; Wnuk, Stanislaw F.
Chemistry Letters, 2011 , vol. 40, # 9 p. 967 - 969
696-62-8
4-碘苯甲醚
+
1350927-23-9
→
反应条件
140-67-0
4-烯丙基苯甲醚
+
1712-69-2
1-异丙烯基-4-甲氧基苯
反应条件
1: With sodium hydroxide in 1,4-dioxane T=20°C; 0.25 h; 2: With palladium diacetate T=95°C; 18 h; chemoselective reaction;
参考文献
Pitteloud, Jean-Philippe; Liang, Yong; Wnuk, Stanislaw F.
Chemistry Letters, 2011 , vol. 40, # 9 p. 967 - 969
90-14-2
1-碘萘
+
1350927-23-9
→
反应条件
1855-47-6
2-异丙苯基萘
+
2489-86-3
反应条件
1: With sodium hydroxide in 1,4-dioxane T=20°C; 0.25 h; 2: With palladium diacetate T=95°C; 18 h; chemoselective reaction;
参考文献
Pitteloud, Jean-Philippe; Liang, Yong; Wnuk, Stanislaw F.
Chemistry Letters, 2011 , vol. 40, # 9 p. 967 - 969