反应条件
Na naphthalide in tetrahydrofuran; toluene
byproducts: NaCl, tBu2PMe, Pt; inert atm.; equimolar ratio, cooling (-78 to 0°C), stirring (10 min), concn. (vac., 20°C), standing (12 h, 20°C); concn. (in 5 h, 20°C), washing (hexane), filtn., evapn. (toluene);
参考文献
Krautscheid; Matern; Kovacs; Fritz; Pikies
Zeitschrift fur Anorganische und Allgemeine Chemie, 1997 , vol. 623, # 12 p. 1917 - 1924