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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
环酯草醚
合成路线
（共 15 条）
113583-35-0
4,6-二甲氧基-2-甲磺酰基嘧啶
+
135217-37-7
→
反应条件
135186-78-6
环酯草醚
反应条件
potassium carbonate in N,N-dimethyl-formamide T=50°C; 2.5 h;
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
13223-25-1
2-氯-4,6-二甲氧基嘧啶
+
135217-37-7
→
反应条件
135186-78-6
环酯草醚
反应条件
potassium carbonate; triphenylphosphine in acetonitrile T=55°C; 23 h;
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
13619-70-0
2-乙酰基-6-硝基苯甲酸
→
反应条件
135186-78-6
环酯草醚
反应条件
1.1: H2 / 5 percent Pd/C / dioxane / 41 h / 30 - 100 °C / 1500.12 Torr 2.1: 37 percent HCl; NaNO2 / H2O / -5 - 0 °C 2.2: potassium xanthogenate; sodium hydroxide / H2O / 0.67 h / 30 - 40 °C 3.1: 90.4 percent / K2CO3 / dimethylformamide / 2.5 h / 50 °C View Scheme
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
335279-63-5
→
反应条件
135186-78-6
环酯草醚
反应条件
1.1: H2 / Raney nickel / tetrahydrofuran; ethanol / 20 h / 25 - 45 °C 2.1: 37 percent HCl; NaNO2 / H2O / -5 - 0 °C 2.2: potassium xanthogenate; sodium hydroxide / H2O / 0.67 h / 30 - 40 °C 3.1: 90.4 percent / K2CO3 / dimethylformamide / 2.5 h / 50 °C View Scheme
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
117-21-5
3-氯苯酐
→
反应条件
135186-78-6
环酯草醚
反应条件
1: Et3N 2: H2 / rhodium catalyst / Heating 3: dimethylformamide / 0.75 h / 100 °C 4: sodium methanethiolate / dimethylformamide / 4 h / 100 - 140 °C 5: 90.4 percent / K2CO3 / dimethylformamide / 2.5 h / 50 °C View Scheme
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
906729-01-9
→
反应条件
135186-78-6
环酯草醚
反应条件
1: H2 / rhodium catalyst / Heating 2: dimethylformamide / 0.75 h / 100 °C 3: sodium methanethiolate / dimethylformamide / 4 h / 100 - 140 °C 4: 90.4 percent / K2CO3 / dimethylformamide / 2.5 h / 50 °C View Scheme
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
148843-77-0
7-氨基-3-甲基苯酞
→
反应条件
135186-78-6
环酯草醚
反应条件
1.1: 37 percent HCl; NaNO2 / H2O / -5 - 0 °C 1.2: potassium xanthogenate; sodium hydroxide / H2O / 0.67 h / 30 - 40 °C 2.1: 90.4 percent / K2CO3 / dimethylformamide / 2.5 h / 50 °C View Scheme
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
13619-67-5
→
反应条件
135186-78-6
环酯草醚
反应条件
1.1: 80.9 percent / NaBH4; NaOH / H2O / 1 h / pH 11 / Heating 2.1: 37 percent HCl; NaNO2 / H2O / -5 - 0 °C 2.2: potassium xanthogenate; sodium hydroxide / H2O / 0.67 h / 30 - 40 °C 3.1: 90.4 percent / K2CO3 / dimethylformamide / 2.5 h / 50 °C View Scheme
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
6833-13-2
2-氯-N-苯基苯甲酰胺
→
反应条件
135186-78-6
环酯草醚
反应条件
1: sec-butyl lithium / -95 °C 2: dimethylformamide / 0.75 h / 100 °C 3: sodium methanethiolate / dimethylformamide / 4 h / 100 - 140 °C 4: 90.4 percent / K2CO3 / dimethylformamide / 2.5 h / 50 °C View Scheme
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
146516-73-6
→
反应条件
135186-78-6
环酯草醚
反应条件
1: dimethylformamide / 0.75 h / 100 °C 2: sodium methanethiolate / dimethylformamide / 4 h / 100 - 140 °C 3: 90.4 percent / K2CO3 / dimethylformamide / 2.5 h / 50 °C View Scheme
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
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