1-(2,3-二脱氧-3-氟-5-O-三苯甲基呋喃戊糖基)-5-甲基-2,4(1H,3H)-嘧啶二酮合成路线 (共 13 条)
反应条件
1: 9.65 g / 0 - 25 °C 2: 70 percent / aq. sodium hydroxide / ethanol / 4 h / Heating 3: N,N-dimethylaminopyridine / dimethylformamide / 4 h / 50 °C 4: diethylaminosulfurtrifluoride / CH2Cl2 / 0 - 25 °C View Scheme
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 23, # 1-2 p. 7 - 29
反应条件
1: N,N-dimethylaminopyridine / dimethylformamide / 4 h / 50 °C 2: diethylaminosulfurtrifluoride / CH2Cl2 / 0 - 25 °C View Scheme
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 23, # 1-2 p. 7 - 29
反应条件
toluene-4-sulfonic acid in methanol; chloroform T=40°C; 0.333333 h;
参考文献
Wilson, I. K.; Chatterjee, S.; Wolf, W.
Journal of Fluorine Chemistry, 1991 , vol. 55, # 3 p. 283 - 289