1,1-二杂苯[B]硫代苯甲基氯草酸酯合成路线 （共 13 条）
反应条件
chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine 1.) CH2Cl2, reflux, 1 h, 2.) 0 deg C 20 min,; room temperature, 1-1.5 h; Yield givenMultistep reaction;
参考文献
Carpino, Louis A.; Ismail, Mohamed; Truran, George A.; Mansour; Iguchi, Shin; Ionescu, Dumitru; El-Faham, Ayman; Riemer, Christoph; Warrass, Ralf
Journal of Organic Chemistry, 1999 , vol. 64, # 12 p. 4324 - 4338
反应条件
1: 74 percent / CH2Cl2 / 20 h 2: 58 percent / Et3N / acetonitrile; H2O / 0.75 h / Ambient temperature; pH 8.5-9 View Scheme
参考文献
Carpino, Louis A.; Ismail, Mohamed; Truran, George A.; Mansour; Iguchi, Shin; Ionescu, Dumitru; El-Faham, Ayman; Riemer, Christoph; Warrass, Ralf
Journal of Organic Chemistry, 1999 , vol. 64, # 12 p. 4324 - 4338
反应条件
chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine
1.) CH2Cl2, reflux, 1 h, 2.) 0 deg C 20 min,; room temperature, 1-1.5 h; Yield givenMultistep reaction;
参考文献
Carpino, Louis A.; Ismail, Mohamed; Truran, George A.; Mansour; Iguchi, Shin; Ionescu, Dumitru; El-Faham, Ayman; Riemer, Christoph; Warrass, Ralf
Journal of Organic Chemistry, 1999 , vol. 64, # 12 p. 4324 - 4338
