2,3-二氢-3-甲基苯并呋喃合成路线 （共 55 条）
参考文献
Gripenberg,J.; Hase,T.
Acta Chemica Scandinavica (1947-1973), 1966 , vol. 20, p. 1561 - 1570
反应条件
[Ru(η4-COD)(η3-methylallyl)2]; BF4(1-)*C27H27N2(1+); potassium tert-butylate; hydrogen in hexane
T=25°C; P=7500.75 Torr; 16 h; Inert atmosphereAutoclave; optical yield given as percent eeenantioselective reaction;
参考文献
Ortega, Nuria; Beiring, Bernhard; Urban, Slawomir; Glorius, Frank
Tetrahedron, 2012 , vol. 68, # 26 p. 5185 - 5192
反应条件
indium(III) chloride; triethyl borane; diisobutylaluminium hydride; oxygen in tetrahydrofuran; hexane
T=20°C; 0.5 h;
参考文献
Takami, Kazuaki; Mikami, Satoshi; Yorimitsu, Hideki; Shinokubo, Hiroshi; Oshima, Koichiro
Tetrahedron, 2003 , vol. 59, # 34 p. 6627 - 6635
反应条件
Sm(III) chloride; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
8 h; Ambient temperatureelectrolysis (Mg anode, Ni foam cathode, constant current 100 mA);
参考文献
Espanet; Dunach; Perichon
Tetrahedron Letters, 1992 , vol. 33, # 18 p. 2485 - 2488
反应条件
triethylsilane; (HS-CH2CH2)-polystyrene
T=70°C; 6 h;
参考文献
Deleuze, Herve; Maillard, Bernard; Mondain-Monval, Olivier
Bioorganic and medicinal chemistry letters, 2002 , vol. 12, # 14 p. 1877 - 1880
反应条件
tetrafluoroboric acid in diethyl ether; dichloromethane
T=0°C; 2 h;
参考文献
Barluenga, Jose; Fananas, Francisco J.; Sanz, Roberto; Marcos, Cesar
Chemistry - A European Journal, 2005 , vol. 11, # 18 p. 5397 - 5407
反应条件
1: K2CO3 / dimethylformamide / 4 h / 70 °C
2: 41 percent / phenanthrene; Et4NClO4; magnesium / dimethylformamide / 0 °C / Electrolysis
View Scheme
参考文献
Kurono, Nobuhito; Honda, Eiichi; Komatsu, Fumikazu; Orito, Kazuhiko; Tokuda, Masao
Tetrahedron, 2004 , vol. 60, # 8 p. 1791 - 1801
反应条件
1: With tert.-butyl lithium in diethyl ether; pentane
T=-78°C; 0.5 h;
2: With N,N,N',N,-tetramethylethylenediamine in diethyl ether; pentane
T=-78°C; 0.5 h; Further stages.;
参考文献
Barluenga, Jose; Fananas, Francisco J.; Sanz, Roberto; Marcos, Cesar
Organic Letters, 2002 , vol. 4, # 13 p. 2225 - 2228
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
T=110°C; P=64600 Torr; 3 h;
参考文献
Ryu, Ilhyong; Niguma, Tatsuro; Minakata, Satoshi; Komatsu, Mitsuo; Hadida, Sabine; Curran, Dennis P.
Tetrahedron Letters, 1997 , vol. 38, # 45 p. 7883 - 7886
反应条件
2,2'-azo-bisisobutyronitrile; α,α,α-trifluorotoluene; (C6F13CH2CH2)3SnH; sodium cyanoborohydride in tert-butyl alcohol
T=90°C; P=60800 Torr; 3 h;
参考文献
Ryu, Ilhyong; Niguma, Tatsuro; Minakata, Satoshi; Komatsu, Mitsuo; Hadida, Sabine; Curran, Dennis P.
Tetrahedron Letters, 1997 , vol. 38, # 45 p. 7883 - 7886
