2,3-二氢-3-甲基苯并呋喃合成路线 (共 55 条)
反应条件
biscyclopentadienyliron(II); tBuCH2CH2B(H)NiPr2 in acetonitrile
T=20°C;
参考文献
Marciasini, Ludovic D.; Richy, Nicolas; Vaultier, Michel; Pucheault, Mathieu
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 6 p. 1083 - 1088
反应条件
sodium tetrahydroborate; 10-methyl-9,10-dihydroacridine in N,N-dimethyl-formamide
Irradiation;
参考文献
Boisvert, Guy; Giasson, Richard
Tetrahedron Letters, 1992 , vol. 33, # 44 p. 6587 - 6590
反应条件
T=413°C; P=135 Torr; 4.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Paul, Gitendra C.; Gajewski, Joseph J.
Journal of Organic Chemistry, 1993 , vol. 58, # 19 p. 5060 - 5062
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene
0.5 h; Heatingother solvent (benzene), other time (5 h); reactions of allyl o-bromoaryl ethers, N-allyl o-bromoacetanilide and related compounds with tributyltin hydride in the presence of activated olefins; Product distribution;
参考文献
Togo, Hideo; Kikuchi, Osamu
Heterocycles, 1989 , vol. 28, # 1 p. 373 - 381
反应条件
oxygen; trimethylamine
P=274 Torr; 8760 h; Ambient temperaturedark;
参考文献
Fornarini, Simonetta; Speranza, Maurizio
Canadian Journal of Chemistry, 1988 , vol. 66, p. 2506 - 2514
反应条件
tetra-n-butylammonium perchlorate; zinc in N,N-dimethyl-formamide
T=25 - 30°C; also other cathodes, other solvents, other electrolytes; also addition of D2O; Product distributionMechanism;
参考文献
Kimura, Makoto; Miyahara, Hiroyoshi; Moritani, Noriyuki; Sawaki, Yasuhiko
Journal of Organic Chemistry, 1990 , vol. 55, p. 3897 - 3902
反应条件
oxygen
P=34 Torr; 8760 h; Ambient temperaturedark; Further byproducts given;
参考文献
Fornarini, Simonetta; Speranza, Maurizio
Canadian Journal of Chemistry, 1988 , vol. 66, p. 2506 - 2514
反应条件
helium; oxygen
P=684 Torr; 8760 h; Ambient temperaturedark; Further byproducts given;
参考文献
Fornarini, Simonetta; Speranza, Maurizio
Canadian Journal of Chemistry, 1988 , vol. 66, p. 2506 - 2514
反应条件
oxygen
P=254 Torr; 8760 h; Ambient temperaturedark; Further byproducts given;
参考文献
Fornarini, Simonetta; Speranza, Maurizio
Canadian Journal of Chemistry, 1988 , vol. 66, p. 2506 - 2514
反应条件
methanol; N,N,N',N,-tetramethylethylenediamine; tert.-butyl lithium
1.) pentane, Et2O, -98 deg C; 2.) pentane, Et2O, 22 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bailey, William F.; Punzalan, Eric R.
Tetrahedron Letters, 1996 , vol. 37, # 31 p. 5435 - 5436