反应条件
1.1: (x)BF4*C9H14NO(1+) / dichloromethane / 1 h / -78 °C
1.2: 20 °C
2.1: N,N,N',N',N'',N''-hexamethylphosphoric triamide; copper(I) bromide dimethylsulfide complex / tetrahydrofuran / 2 h / -78 °C
2.2: 2 h / -78 °C
2.3: 20 °C
3.1: (x)BF4*C9H14NO(1+) / dichloromethane / 1 h / -78 °C
3.2: 20 °C
View Scheme
参考文献
Hayashi, Masaki; Shibuya, Masatoshi; Iwabuchi, Yoshiharu
Organic Letters, 2012 , vol. 14, # 1 p. 154 - 157