反应条件
1.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / -78 - 20 °C / Inert atmosphere
1.2: 48 h / 35 °C / Inert atmosphere
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 20 °C
3.1: tetrachloromethane; potassium hydroxide; tert-butyl alcohol / dichloromethane / 35 - 80 °C
View Scheme
参考文献
Zhou, Hongwei; Xing, Yanpeng; Liu, Le; Hong, Junjie
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 17 p. 3146 - 3150