反应条件
1: 9-bora-bicyclo[3.3.1]nonane; dihydrogen peroxide / tetrahydrofuran / 3 h / Inert atmosphere; Cooling with ice
2: tetrabutyl ammonium fluoride / tetrahydrofuran
3: Jone's reagent / water; acetone / 1 h / 0 °C
4: trifluoroacetic acid / dichloromethane / 20 °C
5: trifluoroacetic acid / dichloromethane / 20 °C
View Scheme
参考文献
CAYMAN CHEMICAL COMPANY, INCORPORATED; ENDRES, Gregory, W.; KORNILOV, Andriy, M.; UZIEBLO, Adam
Patent: WO2011/159740 A2, 2011 ;