1,1,2-三氯-1,2,2-三甲基二硅烷合成路线 （共 23 条）
反应条件
hydrogenchloride T=430 - 750°C; 72 h; Conversion of starting material;
参考文献
US2005/113591 A1, ;
Page/Page column 2 ;
反应条件
hydrogenchloride T=430 - 750°C; 72 h; Conversion of starting material;
参考文献
US2005/113591 A1, ;
Page/Page column 2 ;
反应条件
triphenylphosphine 2 h; Heating; Title compound not separated from byproducts;
参考文献
Matsumoto, Hideyuki; Ohkawa, Kazuhiro; Nakano, Taichi; Nagai, Yoichiro
Chemistry Letters, 1980 , p. 721 - 724
反应条件
1-methyl-1H-imidazole in toluene Product distribution;
参考文献
Herzog; Richter; Brendler; Roewer
Journal of Organometallic Chemistry, 1996 , vol. 507, # 1-2 p. 221 - 228
反应条件
in diethyl ether reaction at -79°C (1 hour), heating to 20°C (8 hours), heating under reflux for 2 hours; further products;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 1.3.3.7, page 17 - 32
反应条件
(i) nBuLi, (ii) /BRN= 2036592/; Multistep reaction;
参考文献
Weidenbruch,M. et al.
Chemische Berichte, 1971 , vol. 104, p. 2124 - 2133
反应条件
hydrogenchloride T=430 - 750°C; 72 h; Conversion of starting material;
参考文献
US2005/113591 A1, ;
Page/Page column 2 ;
反应条件
ZnF2 in 1,1,2,3,4,4-hexachloro-1,3-butadiene T=60 - 70°C; 2 h;
参考文献
Nagy, J.; Zsombok, G.; Hengge, E.; Veigl, W.
Journal of Organometallic Chemistry, 1982 , vol. 232, # 1 p. 1 - 8
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=80°C;
参考文献
Matsumoto, Hideyuki; Kasahara, Miyuki; Matsubara, Ikuya; Takahashi, Masatoshi; Arai, Takeshi; et al.
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 99 - 108
参考文献
Kumada et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 1264,1267
Full Text Show Details
Tokyo Shibaura Electric Co.
Patent: US2881197 , 1953 ;
