1,2-双(氯二甲基硅基)乙烷合成路线 (共 41 条)
反应条件
dihydrogen hexachloroplatinate Heatingdetermination of side products; Product distributionMechanism;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 8 p. 1795 - 1799,1594 - 1597
反应条件
dihydrogen hexachloroplatinate Heating; Product distributionMechanism;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 7 p. 1544 - 1553,1372 - 1381
反应条件
in diethyl ether T=0°C; 5 h;
参考文献
Guggenheim, Thomas L.
Tetrahedron Letters, 1984 , vol. 25, # 12 p. 1253 - 1254
反应条件
triethylamine in dichloromethane 2 h;
参考文献
Leduc; Bernier; Escher
Helvetica Chimica Acta, 1983 , vol. 66, # 3 p. 960 - 970
反应条件
1: K/Na vapor / 280 - 300 °C / 0.1 - 1 Torr 2: 67 percent / O2 View Scheme
参考文献
Adam, Waldemar; Albert, Rainer
Tetrahedron Letters, 1992 , vol. 33, # 52 p. 8015 - 8016
参考文献
Adam, Waldemar; Albert, Rainer
Tetrahedron Letters, 1992 , vol. 33, # 52 p. 8015 - 8016
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) -70 deg C, 20 min, 2.) -70 deg C, 45 min;
参考文献
Grega, Kevin C.; Barbachyn, Michael R.; Brickner, Steven J.; Mizsak, Stephen A.
Journal of Organic Chemistry, 1995 , vol. 60, # 16 p. 5255 - 5261
反应条件
lithium aluminium tetrahydride in bis [2-(2-methoxyethoxy)ethyl] ether T=50°C; 3 h; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 24 p. 4097 - 4100
反应条件
lithium aluminium tetrahydride in diethyl ether 3 h; Heating;
参考文献
Journal of Organometallic Chemistry, , vol. 378, p. 1 - 16
反应条件
triethylamine in dichloromethane 2 h; Ambient temperature;
参考文献
Barrett; Lebold
Tetrahedron Letters, 1987 , vol. 28, # 47 p. 7891 - 5792