反应条件
1: 1.) n-Buli / 1.) room temperature, 4 h, 2.) reflux, 4 h
2: 69 percent / NaOAc, aq. MeCO3H / CH2Cl2 / 3 h / 0 °C
3: 40 percent / aq. HCl / acetone / 1.) 0-5 deg C, 0.5 h, 2.) room temperature, 15 h
4: 64.5 percent / CeCl3*7H2O, NaBH4 / CH2Cl2 / 0.08 h / Ambient temperature
5: 90 percent / basic alumina / diethyl ether / 24 h / Ambient temperature
View Scheme
参考文献
Wang, Zhong-Qi; Zhou, Wei-Shan; Chen, Yi; Wy, Yue-Huan; Zhu, Zhou-Yuan
Synthetic Communications, 1989 , vol. 19, # 19 p. 3267 - 3274
