1-甲基-3-[6-(甲基亚磺酰基)己基]咪唑对甲苯磺酰盐合成路线 （共 5 条）
反应条件
dihydrogen peroxide in tetrahydrofuran; water; acetic acid T=0 - 20°C; 2 h;
参考文献
Tsuchiya, Daisuke; Tabata, Masayuki; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 34 p. 6849 - 6855
反应条件
1.1: thiourea; potassium iodide / ethanol / 14 h / Reflux 1.2: 3 h / Reflux 2.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 °C 3.1: N-Trimethylamine hydrochloride; triethylamine / dichloromethane / 1 h / 0 °C 4.1: acetonitrile / 48 h / 20 - 60 °C 5.1: dihydrogen peroxide / tetrahydrofuran; water; acetic acid / 2 h / 0 - 20 °C View Scheme
参考文献
Tsuchiya, Daisuke; Tabata, Masayuki; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 34 p. 6849 - 6855
反应条件
1: N-Trimethylamine hydrochloride; triethylamine / dichloromethane / 1 h / 0 °C 2: acetonitrile / 48 h / 20 - 60 °C 3: dihydrogen peroxide / tetrahydrofuran; water; acetic acid / 2 h / 0 - 20 °C View Scheme
参考文献
Tsuchiya, Daisuke; Tabata, Masayuki; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 34 p. 6849 - 6855
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 °C 2: N-Trimethylamine hydrochloride; triethylamine / dichloromethane / 1 h / 0 °C 3: acetonitrile / 48 h / 20 - 60 °C 4: dihydrogen peroxide / tetrahydrofuran; water; acetic acid / 2 h / 0 - 20 °C View Scheme
参考文献
Tsuchiya, Daisuke; Tabata, Masayuki; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 34 p. 6849 - 6855
反应条件
1: acetonitrile / 48 h / 20 - 60 °C 2: dihydrogen peroxide / tetrahydrofuran; water; acetic acid / 2 h / 0 - 20 °C View Scheme
参考文献
Tsuchiya, Daisuke; Tabata, Masayuki; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 34 p. 6849 - 6855
