4-甲基-1-戊炔-3-酮合成路线 （共 6 条）
反应条件
Jone's reagent in acetone
参考文献
Mori, Kenji; Tashiro, Takuya; Zhao, Boguang; Suckling, David M.; El-Sayed, Ashraf M.
Tetrahedron, 2010 , vol. 66, # 14 p. 2642 - 2653
反应条件
1: With aluminium trichloride in dichloromethane T=0 - 20°C; 4 h; 2: With tetrabutyl-ammonium chloride; NAF in diethyl ether; water
参考文献
Heiss, Christian; Laivenieks, Maris; Zeikus; Phillips, Robert S.
Bioorganic and Medicinal Chemistry, 2001 , vol. 9, # 7 p. 1659 - 1666
反应条件
tetrabutyl-ammonium chloride; NAF in diethyl ether Hydrolysis;
参考文献
Heiss, Christian; Phillips, Robert S.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2821 - 2825
反应条件
in tetrahydrofuran T=-78 - 20°C; 4 h; Inert atmosphere;
参考文献
Donohoe, Timothy J.; Lacy, Adam R.; Rathi, Akshat H.; Walter, Daryl S.
Chemistry - An Asian Journal, 2011 , vol. 6, # 12 p. 3214 - 3222
反应条件
phosphorus pentachloride in diethyl ether; dichloromethane
Ambient temperature;
参考文献
Naser-Ud-Din; Skattebol, Lars
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 3 p. 247 - 248
反应条件
phosphorus pentachloride in diethyl ether; pentane
Ambient temperaturevarious α-ethynyl ketones; Product distributionMechanism;
参考文献
Naser-Ud-Din; Skattebol, Lars
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 3 p. 247 - 248
