[1R-[1alpha(R*),3abeta,7aalpha]]-八氢-delta,7a-二甲基-4-氧代-1H-茚-1-戊酸甲酯合成路线 (共 6 条)
反应条件
dipyridinium dichromate
参考文献
Mascarenas, Jose L.; Perez-Sestelo, Jose; Castedo, Luis; Mourino, Antonio
Tetrahedron Letters, 1991 , vol. 32, # 24 p. 2813 - 2816
反应条件
lead(IV) acetate in benzene 22 h; Heating;
参考文献
Valles, Maria Jose; Castedo, Luis; Mourino, Antonio
Tetrahedron Letters, 1992 , vol. 33, # 11 p. 1503 - 1506
反应条件
1: 75 percent / CuI, Zn / ethanol; H2O / 0.67 h / Ambient temperature; sonicated 2: 99 percent / pyridinium dichromate View Scheme
参考文献
Mascarenas, Jose L.; Perez-Sestelo, Jose; Castedo, Luis; Mourino, Antonio
Tetrahedron Letters, 1991 , vol. 32, # 24 p. 2813 - 2816
反应条件
1: 89 percent / n-butyllithium / -78 °C 2: 2. tetra-n-butylammonium fluoride / 1. diethyl ether, -78 deg C, 2. THF View Scheme
参考文献
Mascarenas, Jose L.; Perez-Sestelo, Jose; Castedo, Luis; Mourino, Antonio
Tetrahedron Letters, 1991 , vol. 32, # 24 p. 2813 - 2816
反应条件
n-butyllithium T=-78°C;
参考文献
Mascarenas, Jose L.; Perez-Sestelo, Jose; Castedo, Luis; Mourino, Antonio
Tetrahedron Letters, 1991 , vol. 32, # 24 p. 2813 - 2816
反应条件
1: 89 percent / n-butyllithium / -78 °C 2: 2. tetra-n-butylammonium fluoride / 1. diethyl ether, -78 deg C, 2. THF View Scheme
参考文献
Mascarenas, Jose L.; Perez-Sestelo, Jose; Castedo, Luis; Mourino, Antonio
Tetrahedron Letters, 1991 , vol. 32, # 24 p. 2813 - 2816