3-[(4-甲氧基苄基)氧基]-1-丙醇合成路线 （共 16 条）
反应条件
camphor-10-sulfonic acid in dichloromethane; cyclohexane
10 h; Inert atmosphere;
参考文献
Batt, Frederic; Fache, Fabienne
European Journal of Organic Chemistry, 2011 , # 30 p. 6039 - 6055
参考文献
Angle, Steven R.; Bernier, Daniel S.; El-Said, Nahla A.; Jones, Darin E.; Shaw, Stephanie Z.
Tetrahedron Letters, 1998 , vol. 39, # 23 p. 3919 - 3922
反应条件
1: 1.) NaH / 1.) ether, 3.5 h, 2.) 25 deg C, 1 h
2: pyridinium p-toluenesulfonate / Ambient temperature
View Scheme
参考文献
Walkup, Robert D.; Mosher, Michael D.
Tetrahedron, 1993 , vol. 49, # 41 p. 9285 - 9294
反应条件
pyridinium p-toluenesulfonate
Ambient temperature; Yield given;
参考文献
Walkup, Robert D.; Mosher, Michael D.
Tetrahedron, 1993 , vol. 49, # 41 p. 9285 - 9294
反应条件
1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C / |Inert atmosphere
2: tetrahydrofuran / 0.58 h / -78 °C / |Inert atmosphere
3: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.67 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Dieckmann, Michael; Menche, Dirk
Organic Letters, 2013 , vol. 15, # 1 p. 228 - 231
反应条件
manganese(IV) oxide; sodium hydrogencarbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone in nitromethane
T=20°C; 40 h; Inert atmosphereMolecular sieve;
参考文献
Liu, Lei; Floreancig, Paul E.
Organic Letters, 2010 , vol. 12, # 20 p. 4686 - 4689
