[(2S,3Z)-2-羟基-3-(5-氧代呋喃-2-亚基)丙基]苯甲酸酯合成路线 （共 6 条）
反应条件
triethylamine in tetrahydrofuran
T=-40°C; 2 h;
参考文献
Shen, Chien-Chang; Chou, Shiu-Ching; Chou, Cheng-Jen; Ho, Li-Kang
Tetrahedron Asymmetry, 1996 , vol. 7, # 11 p. 3141 - 3146
反应条件
triethylamine in tetrahydrofuran
T=-40°C; 2 h;
参考文献
Pohmakotr, Manat; Tuchinda, Patoomratana; Premkaisorn, Pornchai; Limpongpan, Attasit; Reutrakul, Vichai
Heterocycles, 1999 , vol. 51, # 4 p. 795 - 802
反应条件
in dichloromethane
T=-10°C;
参考文献
Lu, Xiyan; Chen, Guoying; Xia, Lijun; Guo, Guangzhong
Tetrahedron Asymmetry, 1997 , vol. 8, # 18 p. 3067 - 3072
反应条件
triethylamine in dichloromethane
Yield givenTitle compound not separated from byproducts;
参考文献
Pohmakotr, Manat; Tuchinda, Patoomratana; Premkaisorn, Pornchai; Limpongpan, Attasit; Reutrakul, Vichai
Heterocycles, 1999 , vol. 51, # 4 p. 795 - 802
反应条件
triethylamine in dichloromethane
in refrigerator, 22 h;
参考文献
Pohmakotr, Manat; Tuchinda, Patoomratana; Premkaisorn, Pornchai; Limpongpan, Attasit; Reutrakul, Vichai
Heterocycles, 1999 , vol. 51, # 4 p. 795 - 802
反应条件
1: 57 percent / 90 percent TFA / 26 h / 0 °C
2: 60 percent / Et3N / tetrahydrofuran / 2 h / -40 °C
View Scheme
参考文献
Pohmakotr, Manat; Tuchinda, Patoomratana; Premkaisorn, Pornchai; Limpongpan, Attasit; Reutrakul, Vichai
Heterocycles, 1999 , vol. 51, # 4 p. 795 - 802
