3-(4-氯苯基)-1H-吡唑-4-羧酸合成路线 （共 5 条）
反应条件
sodium hydroxide; potassium permanganate in water T=20 - 98°C;
参考文献
Lebedev; Lebedeva; Sheludyakov; Kovaleva; Ustinova; Kozhevnikov
Russian Journal of General Chemistry, 2005 , vol. 75, # 5 p. 782 - 789
反应条件
1: 32 percent / POCl3 / 40 - 80 °C 2: 95 percent / NaOH; KMnO4 / H2O / 20 - 98 °C View Scheme
参考文献
Lebedev; Lebedeva; Sheludyakov; Kovaleva; Ustinova; Kozhevnikov
Russian Journal of General Chemistry, 2005 , vol. 75, # 5 p. 782 - 789
反应条件
1.1: AcONa / ethanol / 0.75 h / Heating 1.2: ethanol / 1 h / Heating 2.1: 32 percent / POCl3 / 40 - 80 °C 3.1: 95 percent / NaOH; KMnO4 / H2O / 20 - 98 °C View Scheme
参考文献
Lebedev; Lebedeva; Sheludyakov; Kovaleva; Ustinova; Kozhevnikov
Russian Journal of General Chemistry, 2005 , vol. 75, # 5 p. 782 - 789
反应条件
1: CH2Cl2; diethyl ether / 24 h / Ambient temperature 2: 1.) Br2, 2.) conc. HCl / 1.) CH2Cl2,, RT, 30 min, 2.) reflux, 1 d View Scheme
参考文献
Nakano, Yoshihiko; Ilamaguchi, Masashi; Nagai, Toshikazu
Journal of Chemical Research, Miniprint, 1991 , # 7 p. 1701 - 1757
反应条件
in diethyl ether; dichloromethane 0.166667 h; Ambient temperature;
参考文献
Nakano, Yoshihiko; Ilamaguchi, Masashi; Nagai, Toshikazu
Journal of Chemical Research, Miniprint, 1991 , # 7 p. 1701 - 1757
