(2E)-3-(4-甲基苯基)丙烯酰氯合成路线 (共 4 条)
反应条件
thionyl chloride in cyclohexane 3 h; Heating;
参考文献
SENOMYX, INC.; PRIEST, Chad; NONCOVICH, Alain; PATRON, Andrew; UNG, Jane
Patent: WO2012/61698 A2, 2012 ;
Location in patent: Page/Page column 95 ;
WO 2012/061698 A2
反应条件
in dichloromethane; chloroform; N,N-dimethyl-formamide T=20°C; 2 h;
参考文献
King, Frank D.; Caddick, Stephen
Tetrahedron, 2013 , vol. 69, # 2 p. 487 - 491
反应条件
1.1: pyridine; piperidine 1.2: HCl / Heating 2.1: thionyl chloride / 20 °C View Scheme
参考文献
Li, Dong-Dong; Lv, Peng-Cheng; Zhang, Hui; Zhang, Hong-Jia; Hou, Ya-Ping; Liu, Kai; Ye, Yong-Hao; Zhu, Hai-Liang
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 16 p. 5012 - 5022
反应条件
T=25°C; kinetic isotope effect; var. solvents; Rate constant;
参考文献
Kim, Tae-Hyoung; Huh, Chul; Lee, Bon-Su; Lee, Ikchoon
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 12 p. 2257 - 2262