in methanol byproducts: HNO3; complex prepd. at room temp. by slow diffusion of two methanol solns.; one soln. containing cis-CrF2(phen)2(NO3) and other - Dy(NO3)3*nH2O; total time of synthesis 6-12 mo; crystals sepd. from powder DyF3 and washed by decantation with methanol;elem. anal., XRD;
参考文献
Journal of Physical Chemistry A, , vol. 116, # 30 p. 7842 - 7847
LiF; NaF in melt byproducts: LiDyF4, NaDyF4; heating of DyF3 and Zr in molten mixt. of 39 mol percent NaF and 61 mol percent LiF at 465 - 625°C; monitoring by differential thermal XRD and IR;
参考文献
Savchuk; Nagornyi; Kompanichenko; Omel'chuk
Russian Journal of Inorganic Chemistry, 2003 , vol. 48, # 10 p. 1454 - 1458
